Description

Chromatograph «Crystallux–4000M» serves as a base for creation of the laboratory analytical systems, designed for the researching and production routine tasks:

Composition and quality analysis of natural gas, incidental gas, dissolved gas and gas condensate with evaluation of heating ability, relative and total density, pressure of saturated steam;
Detailed and group analysis of the gasoline with evaluation of octane number, density, fraction composition, saturated steam pressure, etc.;
Analysis of motor fuel on the content of aromatic and oxygen-containing compounds, MMA, etc.;
Motor fuel, oil and gas analysis on content of and hydrogen sulphide, mercaptans, sulphides, thiophenes and other sulphides;
Analysis of chemical and petrochemical products;
Analysis of transformer oil for content of dissolved gases, water, total gas content, antioxidant admixtures, furan derivatives, polychlorinated biphenyl, insulating gas analysis;
Analysis of the authenticity of alcoholic beverages, including cognacs;
Analysis of wine and wine materials for content of ethanol, organic acids and other admixtures;
Analysis of water for the content of volatile halogen-containing and aroma compounds, acetone, methanol, saturated hydrocarbons, mineral oils, etc.;
Analysis on content of pesticides, herbicides and other toxicants in water, soil, crop products and food;
Analysis of atmosphere air on content of halogenated and aromatic hydrocarbons, carbon oxides, etc;
Analysis of production exhausts and of working area air on containing of saturated, unsaturated and aroma hydrocarbons, carbon oxides, etc.;
Analysis of toxicity of food products packages, building materials and other domestic materials including toys;
Analysis of mine air on content of constant gases, carbon oxides and hydrocarbons;
Analysis of quality of vegetable and animal oils, dairy produce margarines, spreads, milk products, detection of falsification;
Analysis of biological liquids and tissues of human body for contents of alcohol, drugs, medicaments and poisonous substances;
Analysis of gas environment of nuclear power stations;
Analysis of products of blast furnace production, quality of gases, used in metallurgy;
Analysis of impurities in helium, oxygen, nitrogen, argon by cryogenic concentration method;
Analysis of oil and chemical reagents for its production on content of volatile organochlorine compounds;
Analysis of products of color industry;
Analysis of quality of tobacco products;
Analysis of propellents, aerosols, coolagents;
Analysis of adsorbed gases in soil for geologist researches of oils and gas.
Design
Chromatograph is fully automated, starting from injection of a sample and ending with processing of chromatograph information, at that number — functions of automatic control the thermostat temperature, gas-carrier consumption and pressure of auxiliary gases, detector automatic lighting, flame burning control, measuring the signals from detectors with 24—digit ADC.
One computer can work in real time with several analytical modules up to 8, besides, control the operation and process the chromatography signals «Crystall—2000», «Crystallux—4000», process the chromatograph signals through other marks through ADC. Information transfer between computer, analytical station, and chromatographs are performed by the standard interface RS-232, USB. There are control desk of chromatograph on base of microcomputer Pocket PC. Control of chromatograph is possible from the distance up to 3000 m, and also remote control and diagnostics of the chromatograph via the Internet.

Replaceable modules
Replaceable analytical module, installed on the column thermostat, determines the chromatograph model and includes detectors (multidetector), injectors and additional devices. The module configuration can be chosen by the customer for the certain analysis conditions.

Module FID/FID
Module TCD(TCD/TCD)
Module FID/TCD (FID/TCD/TCD)
Module ECD/TID (FID/ECD/TID)
Module PID (PID/ECD, PID/FID)
Module FID/ECD/NPD (FID/NPD)
The modules include two (three) injectors, which can be transformed from capillary into packed type by installing special adapters. On the customer request we can supply module with any detector set and sample input devices: PID/TCD, FID/ECD/PID, TCD/FPD, TCD/TCD/FPD, FID/FID/ECD, FID/ECD/ECD, FID/FID/TCD, HID, FID/FID/FID, TCD/TChD etc.).

Replaceable analytical devices:
Research and production company “Meta-chrom” provides setup and installation, staff training, mounting of gas-chromatography laboratories, service, implementation of methods, modernization of chromatographs “Crystall-2000”, “Crystallux-4000” by increasing of sensitivity, stability and reliability of operation.

Chromatograph could be supplied in set with add-on analytical devices by customer request:

Automated sampler of liquid samples of HT-3000А type, it is differed with possibility of sample injecting one by one into both injectors, injecting a sample with inner standard, free injector for manual injection;
Valve for switching columns;
Headspace sampler HT2000H (Italy) for equilibrium vapor samples;
Combined autosampler HT2800T (liquid, equilibrium vapor, SPME);
Gas injection valves from 4 to 12 steps, including automated and thermostated, working temperature of valves is up to 180 °C ;
Backflush valve, also automated;
Liquified gas sampler, also automated and cooled to minus 5 °C;
Automated capillary column switching device with the help of Dean elements;
Pyrolyzer;
Methanator for analysis of СО, СО2;
Device for cooling of column thermostat, also without use of refrigerant;
Thermodesorber, with possibility of solid sample input;
Equilibrium vapor dispenser;
Catalytic purification filter (nitrogen from oxygen, air from hydrocarbons) separately and in one corpus;
Device for achieving of balance in transformer oil;
Device for cryoconcentration;
PC;
Nitrogen, hydrogen, air generators;
Gas panel, etc.
If the purchaser owns non-automated chromatographs like “LHM-80”, “Model 3700”, “Tsvet” series and others, including foreign chromatographs of old type, there is possibility to upgrade and automatize processing of chromatographic signal with the help of hardware and software complex of “Meta-chrom” on the basis of 24-bit multi-channel ADC (up to 8 channels), that includes PC and program “NetChrom”. Logarithmic digital current meter with possibility to measure current signal in the range from 1x10-14 to 5x10-7A without switching of limits is supplied to replace FID amplifier of old models of chromatographs like IMT-0,5. This complex is included in the State registry of measuring instruments №25150-03, certificate RU.C.31.003. A №15342 from 20.08.09.

General characteristics of ADC and GFG
Possibility to automatize gas flows (from 1 to 5 channels) by consumption and pressure with the help of Gas flow generator “Meta-chrom” if the purchaser owns non-automated chromatographs like “LHM-80”, “Model 3700”, “Tsvet” series, “Chrom” and others, including foreign chromatographs of old type.

Specification

1. Specification_RUS_ENG.docx